Reaction Screening Using a Microreactor

FH – HES

Authors

  • Olivier Naef Ecole d'Ingénieurs et d'architectes de Fribourg Boulevard de Pérolles 80, CP 32, CH-1705 Fribourg
  • Mathieu Roch
  • Thierry Chappuis

DOI:

https://doi.org/10.2533/chimia.2010.889

Keywords:

Continuous mode, Esterification, Microreactor, Optimization, Screening

Abstract

This article discusses the screening of chemical reactions using a microreactor equipped with infrared spectroscopy as online analytics. An esterification reaction has been optimized in continuous mode with the proposed setup. The esterification did not work well due to the material of the microreactor (stainless-steel 316Ti) that catalyzed the decomposition of formic acid. However, despite the occurrence of decomposition, an optimization could be achieved with this system.

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Published

2010-12-15