Determination of Heats of Reaction under Refluxing Conditions

Authors

  • Jacques Wiss
  • Francis Stoessel
  • Gerard Killé

DOI:

https://doi.org/10.2533/chimia.1990.401

Abstract

The accuracy of thermal measurements under reflux conditions strongly depends on the experimental conditions. The temperature difference TJ–TR imposed on the system and the temperature of the reactor lid and reflux equipment play an important role. The optimization of these parameters and their use in the evaluation of different chemical model reactions is shown.

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Published

1990-12-19